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mercur - Atomic fluorescence spectrometer for mercury determination

 mercur - the atomic fluorescence spectrometer from Analytik Jena to the sup-ppt level

mercur is a compact system specially optimized for the complete, cost-efficient determination of mercury traces.

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At first glance:

  • Highly automated - in combination with an autosampler and easy to operate, it meets all expected requirements from a modern routine analysis system with highest sample throughput
  • Fast - thanks to continuous flow operation with or without autosampler plus the unique FBR routine (Fast Baseline Return)
  • Safe - through the use of a bubble sensor, a specially optimized drying membrane, and cascade enrichment
  • Efficient ? due to automated, intelligent gas-liquid control, ensuring minimum reagent consumption and short measurement times in various operating modes
  • Best detection limits - through simple or cascade enrichment
  • Compliant to EN/DIN and EPA-regulations

Clever dosage
Pump systems separately meter sample and reagents and transport them to the reactor. The reductant is fed directly into the reactor. There the two solutions meet at an acute angle. The resulting chemical reaction immediately releases atomic mercury vapor. This mode of separating sample and acid ensures fast cleaning of the pump tubing after aspiration of the sample solution. This helps to save time and reduces the amount of reagents needed. It additionally prevents contamination in case of large concentration gradients within a sequence of measurements.

Intelligent control
To ensure a smooth reaction process in any of the various operating modes, the mercur features an intelligent gas/liquid control system. Thanks to the instrument`s complex valve groups, tubing paths have been minimized to prevent contamination, and to keep carry-over as low as possible. The system-flushing feature and the intelligent gas/liquid control system are responsible for a smooth reaction process and operating whenever the calibrated concentration range is exceeded. This guarantees a successful analysis in cases of strong variations of the mercury content within a sequence of measurements. These features are needed in order to take advantage of the wide linear range of the atomic fluorescence spectrometer in everyday routine analysis.

Optimum enrichment
To adapt the mercur to varied analytical tasks, you can choose between three enrichment modes: no enrichment, simple enrichment, and cascade enrichment. The cascade enrichment feature, compliant to EPA 1631 requirements, comprises two coupled gold collectors, which ensures clean separation of the matrix and prevents quenching effects - thus providing maximum dependability even with complex samples. Enrichment times can be varied to match the sample matrix or the expected mercury concentration range.

Efficient protection
The mercur displays its true strength when handling complicated samples such as foaming solutions. These occur frequently in everyday laboratory practice and involve a high risk of contamination and carry-over. The mercur features an important detail that helps avoid unnecessary cleaning: the Bubble Sensor. If a liquid threatens to spill into the system, this sensor causes the valves to close, and the liquid is automatically conducted to the waste container. Positioned between gas-liquid separator and drying membrane, it protects the gold collector and the fluorescence cell against contamination.

 

 AnalytikJena UK